Bio-Based Surface Engineering of AISI 316L for Durable Electromedical Devices
DOI:
https://doi.org/10.55981/jet.853Keywords:
AISI 316L stainless steel, bio-based carburizing, surface hardness, diffusion layer, sustainable surface engineeringAbstract
This study investigates a bio-based pack carburizing treatment for AISI 316L austenitic stainless steel using an environmentally friendly carburizing mixture composed of 70% Alaban wood charcoal and 30% eggshell powder. The treatment was conducted to improve the surface properties of AISI 316L for potential use in non-implant metallic components of electromedical devices. Solid-state pack carburizing was performed at 600 °C, 700 °C, and 800 °C for 3 h. The treated specimens were evaluated in terms of surface carbon content, microstructural changes, diffusion layer thickness, surface hardness, and hardness distribution. The results showed that increasing carburizing temperature enhanced carbon absorption and surface modification. The highest surface carbon content of 0.80% was obtained at 800 °C. At the same temperature, the surface hardness increased to 346 HV, and the maximum diffusion layer thickness reached 16.7 µm. Microstructural observations revealed the gradual formation of a darker and more continuous carbon-enriched modified layer as the carburizing temperature increased. These improvements indicate that the treated surface became more resistant to localized deformation, repeated contact, and light friction, which are important factors for maintaining the durability and functional reliability of metallic parts in electromedical devices. These findings indicate that the Alaban wood charcoal–eggshell powder mixture can act as an effective bio-based carburizing medium for improving the surface durability of AISI 316L stainless steel. Therefore, the proposed treatment not only enhances the surface performance of AISI 316L but also offers a sustainable and low-cost surface engineering approach for non-implant electromedical components exposed to repeated handling, cleaning, and maintenance activities.
Downloads
References
[1] S. Adachi, T. Yamaguchi, K. Tanaka, T. Nishimura, and N. Ueda, “Effects of solid-solution carbon and eutectic carbides in aisi 316l steel-based tungsten carbide composites on plasma carburizing and nitriding,” Metals (Basel)., vol. 13, no. 8, p. 1350, 2023, doi: 10.3390/met13081350.
[2] R. Montanari et al., “Plasma carburizing of laser powder bed fusion manufactured 316 l steel for enhancing the surface hardness,” Coatings, vol. 12, no. 2, p. 258, 2022, doi: 10.3390/coatings12020258.
[3] G. Park et al., “Effect of carburization on the microstructure and laser weldability of 316l stainless steel,” J. Weld. Join., vol. 41, no. 6, pp. 475–485, 2023, doi: 10.5781/JWJ.2023.41.6.7.
[4] Suprapto, T. Sujitno, D. Slamet Pudjorahardjo, H. Suprihatin, I. Zulhendri, and Saefurrochman, “Thin film deposition of tungsten nitride on ss 316 l surface using dc-sputtering technique,” in J. Phys. Conf. Ser., 2023, vol. 2498, no. 1, p. 12019, doi: 10.1088/1742-6596/2498/1/012019.
[5] Y. Lee et al., “Rapid and scalable lubrication coating for industrial and medical applications via sequential dip‐coating,” Adv. Mater. Interfaces, vol. 12, no. 14, p. e00353, 2025, doi: 10.1002/admi.202500353.
[6] E. Bolli et al., “Surface characteristics and tribological behavior of 3d-printed 316 l steel after plasma assisted low temperature carburizing,” Surf. Coatings Technol., vol. 477,p. 130295, 2024, doi:10.1016/j.surfcoat.2023.130295.
[7] R. Guardian-Tapia, I. Rosales-Cadena, J. L. Roman-Zubillaga, and S. R. Gonzaga-Segura, “Mechanical and microstructural characterization of aisi 316l stainless steel superficially modified by solid nitriding technique,” Coatings, vol. 14, no. 9, p. 1167, 2024, doi: 10.3390/coatings14091167.
[8] H. Yan, L. Zhao, Z. Chen, X. Hu, and Z. Yan, “Investigation of the surface properties and wear properties of aisi h11 steel treated by auxiliary heating plasma nitriding,” Coatings, vol. 10, no. 6, p. 528, 2020, doi: 10.3390/coatings10060528.
[9] Ramli and C.-C. Wu, “Effective case depth and wear resistance of pack carburized scm 420 steel processed using different concentrations of natural shell waste powders and carburizing duration,” Crystals, vol. 12, no. 2, p. 296, 2022, doi: 10.3390/cryst12020296.
[10] H. L. Che, X. Yang, H. Y. Liu, and M. K. Lei, “Gradient self-organized dislocation in expanded austenite layer during low-temperature nitriding,” Mater. Res. Express, vol. 10, no. 7, p. 76512, 2023, doi: 10.1088/2053-1591/ace6f9.
[11] A. Robittah, W. Suprapto, T. D. Widodo, W. A. Wirawan, and A. Sabitah, “ECO–innovative carburizing: enhancing steel st 37 with alaban charcoal and eggshell catalysts,” Int. J. Mech. Eng. Technol. Appl., vol. 6, no. 1, pp. 121–132, 2025, doi: 10.21776/MECHTA.2025.006.01.13.
[12] F. Du et al., “Laser cladding of inconel 718 coating on stainless steel surface,” Phys. Scr., vol. 100, no. 3, p. 35943, 2025, doi: 10.1088/1402-4896/adb34f.
[13] E. P. R. de Oliveira, R. R. de Oliveira, J. G. Vicente, M. Massi, and A. A. Couto, “Induced residual stress in austenitic stainless steel f138 after shot peening and plasma nitriding surface treatment,” in Defect Diffus. Forum, 2025, vol. 439, pp. 147–156.
[14] A. Karim, I. Azmy, S. Q. Khoiriah, and C. Bintoro, “Microstructure and mechanical properties of pack carburized aisi 1020 steel using na2co3 and caco3 catalysts,” J. Renew. Energy Mech., vol. 5, no. 02, pp. 52–59, 2022, doi: 10.25299/rem.2022.vol5.no02.9965.
[15] R. Adawiyah, N. Rahman, A. Sabitah, I. N. Ardiyat, and A. Robittah, “Analisis kandungan karbon dan kekerasan baja aisi 1020 dengan variasi media karburasi batubara lignit dan cangkang telur,” J. Rekayasa Mesin, vol. 19, no. 3, pp. 431–438, 2024, doi: 10.32497/jrm.v19i3.5937.
[16] F. Borgioli, E. Galvanetto, and T. Bacci, “Effects of surface modification by means of low-temperature plasma nitriding on wetting and corrosion behavior of austenitic stainless steel,” Coatings, vol. 10, no. 2, p. 98, 2020, doi: 10.3390/coatings10020098.
[17] D. Tang et al., “High-efficient gas nitridation of aisi 316l austenitic stainless steel by a novel critical temperature nitriding process,” Coatings, vol. 13, no. 10, p. 1708, 2023, doi: 10.3390/coatings13101708.
[18] L. Sun, Y. Li, C. Cao, G. Bi, and X. Luo, “Effect of low-temperature plasma carburization on fretting wear behavior of aisi 316l stainless steel,” Coatings, vol. 14, no. 2, p. 158, 2024, doi: 10.3390/coatings14020158.
[19] N. Chatti, A. Zaidi, H. Makhlouf, M. Lajnef, and L. Lakhal, “Create sustainable competitive advantage and improve sustainable performance by implementing lean and green manufacturing practices: an empirical study on german manufacturing smes,” Int. J. Product. Perform. Manag., vol. 75, no. 1, pp. 153–179, 2026, doi: 10.1108/IJPPM-05-2024-0298.
[20] A. Mathur and P. S. Bahadur, “Laser‐Assisted green manufacturing: advancing environmental sustainability,” Laser Mater. Process. Manuf. Tech., pp. 301–322, 2026, doi: https://doi.org/10.1002/9781394398799.ch11.
[21] Y. Singh and N. K. Singh, “Additives in green manufacturing: mechanisms, applications, and performance,” Green Manuf. with Artif. Intell. Appl., 1st ed, Germany, Berlin, 2026, p. 167-184.
[22] A. Achmadi, T. D. Widodo, and Y. S. Irawan, “Influence of lorjuk mussel shells and peanut shells as carburizer media in the pack carburizing process of aisi 1020,” Int. J. Mech. Eng. Technol. Appl., vol. 6, no. 1, pp. 34–47, 2025, doi: https://doi.org/10.21776/MECHTA.2025.006.01.4.
[23] M. Rafi, I. G. K. Puja, and R. Rines, “The role of nanocatalyst of pearl oyster shell in pack carburizing process on mechanical and physical properties of aisi 1020 steel,” in E3S Web Conf., 2024, vol. 475, p. 1002, doi: 10.1051/e3sconf/202447501002.
[24] H. Boumediri et al., “Effect of carburizing time treatment on microstructure and mechanical properties of low alloy gear steels,” Mater. Res. Express, vol. 11, no. 7, p. 76505, 2024, doi: 10.1088/2053-1591/ad5cd6.
[25] Ramli and C.-C. Wu, “Novel study on mechanical properties of pack carburizing scm 420 steel with energizer dog conch,” Int. J. Mod. Phys. B, vol. 35, no. 05, p. 2150065, 2021, doi: 10.1142/S021797922150065X.
[26] S. Kusmanov et al., “Increasing hardness and wear resistance of austenitic stainless steel surface by anodic plasma electrolytic treatment,” Metals (Basel)., vol. 13, no. 5, p. 872, 2023, doi: 10.3390/met13050872.
[27] G. He et al., “The carburizing behavior of high‐temperature short‐time carburizing gear steel: effect of nb microalloying,” Steel Res. Int., vol. 93, no. 11, p. 2200427, 2022, doi: 10.1002/srin.202200427.
[28] Ramli, C.-C. Wu, and A. Shaaban, “Mechanical properties of pack carburized scm 420 steel processed using natural shell powders and extended carburization time,” Crystals, vol. 11, no. 9, p. 1136, 2021, doi: 10.3390/cryst11091136.
[29] K. D. Ambiger et al., “Influence of gas carburization on the microstructure, mechanical properties, and alloying elements behaviour in plain and alloyed low carbon steels,” Mater. Res. Express, vol. 12, no. 4, p. 46507, 2025, doi: 10.1088/2053-1591/adc9fe.
[30] P. D. Setyawan, I. Hakiki, S. Sugiman, S. Salman, S. Sinarep, and A. Maulana, “Hybrid spot welding-epoxy bonding of aisi 1008 steel: shear and nugget analysis,” J. Polimesin, vol. 23, no. 5, pp. 611–621, 2025, doi: 10.30811/jpl.v23i5.7487.
[31] S. Sinarep and S. Darmo, “Effect of pack carburizing with chicken egg shell powder agent and vibrator quenching on the mechanical properties of aisi 9310 steel,” Eastern-European J. Enterp. Technol., vol. 6, no. 12, p. 114, 2021, doi: 10.15587/1729-4061.2021.244118.
[32] W. D. Callister Jr. and D. G. Rethwisch, Callister’s materials science and engineering, 10th ed, Hoboken, NJ: John Wiley & Sons, 2020.
[33] W. D. Callister Jr. and D. G. Rethwisch, Fundamentals of materials science and engineering, 6th ed, Hoboken, NJ: John Wiley & Sons, 2022.
[34] S. Liu, Z. Yang, T. Liu, Z. Li, and T. Cong, “Effect of case depth and hardness distribution on the rolling contact fatigue performance of g20crni2moa carburized steel,” Steel Res. Int., vol. 95, no. 6, p. 2300875, 2024, doi: 10.1002/srin.202300875.
[35] A. H. Isahak, M. F. Abdullah, M. K. Faidzi, and S. Abdullah, “Effect of microstructure and surface diffusion on crack resistance of low-carbon steel using oil-based cnt nanofluid quenching,” J. Fail. Anal. Prev., pp. 1–15, 2026, doi: 10.1007/s11668-026-02432-7.
[36] C. Liang, P. Cheng, and C. Shao, “Physics-informed machine learning for predicting carburizing process outcomes in 20cr2ni4 steel: a cascade modeling approach,” Metals (Basel)., vol. 16, no. 2, p. 163, 2026, doi: 10.3390/met16020163.
[37] M. A. Ballem, M. M. Aldarwish, A. S. Aljuroushi, A. M. Shaka, and A. M. Abdulbakee, “Effect of carburizing temperature and post carburizing treatments on microhardness and microstructural evolution of carburized low-carbon steel,” J. Pure Appl. Sci., vol. 22, no. 2, pp. 68–72, 2023, doi: 10.51984/jopas.v22i2.2788.
[38] Y. E. Jeong, J. Y. Lee, E. K. Lee, and D. S. Shim, “Microstructures and mechanical properties of deposited fe-8cr-3v-2mo-2w on scm420 substrate using directed energy deposition and effect of post-heat treatment,” Materials (Basel)., vol. 14, no. 5, p. 1231, 2021, doi: 10.3390/ma14051231.
[39] X. Zhang et al., “High-temperature carburization of gear steels: grain size regulation, microstructural evolution, and surface performance enhancement,” Coatings, vol. 16, no. 3, p. 386, 2026, doi: 10.3390/coatings16030386.
[40] G. Zhang et al., “High-temperature oxidation and carburization, corrosion protection, materials selection and coolant chemistry for supercritical carbon dioxide power cycles: a review,” Int. Mater. Rev., vol. 71, no. 1, pp. 30–94, 2026, doi: 10.1177/09506608251369099.
[41] C. Fang, Y. Zhang, W. Liao, X. Leng, and H. Chen, “High-temperature corrosion behavior of structural materials in supercritical carbon dioxide,” J. Mater. Sci., vol. 61, no. 1, pp. 51–75, 2026, doi: 10.1007/s10853-025-11965-5.
[42] J. Zuo, W. Wang, and X. Zhang, “Study on vacuum gas nitriding process and surface properties of aisi 430 stainless steel,” Surf. Sci. Technol., vol. 4, no. 1, p. 10, 2026, doi: 10.1007/s44251-025-00111-7.
[43] S. Baali, Y. Benarioua, and A. E. Mazouz, “An experimental study of the influence of carburizing treatment holding time on the structure and hardness of 16nc6 steel,” Eng. Technol. Appl. Sci. Res., vol. 13, no. 2, pp. 10478–10482, 2023, doi: 10.48084/etasr.5684.
[44] Z. Zhang, Z. Wu, Y. Yuan, X. Wang, and Y. Tian, “Microstructure evolution and mechanical properties of high-temperature carburized 18cr2ni4wa steel,” Materials (Basel)., vol. 17, no. 19, p. 4820, 2024, doi: 10.3390/ma17194820.
[45] G. He, S. Wan, B. Jiang, Z. Wang, Y. Liu, and C. Wu, “Enhanced toughness of high‐temperature carburizing gear steel via refining twin martensite and retained austenite by nb microalloying,” Steel Res. Int., vol. 93, no. 11, p. 2200425, 2022, doi: 10.1002/srin.202200425.
[46] H. Zhang, J. Wu, Z. Qin, and Y. Luo, “The effect of bio-oil on high-temperature performance of bio-oil recycled asphalt binders,” J. Renew. Mater., vol. 10, no. 4, p. 1025-1037, 2022, doi: 10.32604/jrm.2022.017483.
[47] K. V Werner, H. L. Che, M. K. Lei, T. L. Christiansen, and M. A. J. Somers, “Low temperature carburizing of stainless steels and the development of carbon expanded austenite,” HTM J. Heat Treat. Mater., vol. 77, no. 1, pp. 3–15, 2022, doi: 10.1515/htm-2022-0001.
[48] Z. Liu et al., “Effect of low-temperature gaseous carburizing on the compression behavior of 316 l lattice structures manufactured via laser powder bed fusion,” Mater. Des., p. 116070, 2026, doi: 10.1016/j.matdes.2026.116070.
[49] X. Qin, “Hydrogen embrittlement of austenitic stainless steels influence of hydrogen charging, microstructure and low-temperature carburizing.” Ph.D. dissertation, Chalmers Tekniska Hogskola, Sweden, 2026.
Downloads
Published
Issue
Section
License
Copyright (c) 2026 National Research and Innovation Agency

This work is licensed under a Creative Commons Attribution-NonCommercial-ShareAlike 4.0 International License.
Authors who publish with this journal agree to the following terms:
The copyright to this article is transferred to BRIN if and when the article is accepted for publication. The undersigned hereby transfers any and all rights in and to the paper including without limitation all copyrights to BRIN. The undersigned hereby represents and warrants that the paper is original and that he/she is the author of the paper, except for material that is clearly identified as to its original source, with permission notices from the copyright owners where required. The undersigned represents that he/she has the power and authority to make and execute this assignment. The copyright transfer form can be downloaded here.
The corresponding author signs for and accepts responsibility for releasing this material on behalf of any and all co-authors. This agreement is to be signed by at least one of the authors who have obtained the assent of the co-author(s) where applicable. After submission of this agreement signed by the corresponding author, changes of authorship or in the order of the authors listed will not be accepted.

This work is licensed under a Creative Commons Attribution-NonCommercial-ShareAlike 4.0 International License.


